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How to select DPT (Dye Penetrant Testing) Chemicals
Dye Penetrant Inspection (DP) is a process which is applicable for the detection of discontinuities such as lack of fusion, corrosion, cracks, laps, cold shuts, porosity that are open or connected to the surface of the component under examination with the utilization of 3 Major Chemicals: Penetrant, Developer & Cleaner. Also known as Liquid Penetrate Inspection (LPI) or Penetrant Testing (PT), it is a widely used as low-cost inspection method used to check surface-breaking defects in all non-porous materials (metals, plastics or ceramics).

Let’s look at some of the major factors which influence the operator’s choice of Selection of Penetrant, Developer & Cleaner.
Penetrant Selection
Factors which specify the quality of a penetrant and further influence the authenticity of inspection are:

Viscosity: The viscosity of penetrant should not be higher than 3.0 cSt at 38°C/100°F and not more than 5.0 cSt at the lowest temperature, as higher the viscosity slower rate of penetration & lower the viscosity penetrant drain away easily.

Capillarity: Capillarity is the ability of liquid to rise & fall in a narrow opening, hence cavities which offer narrow openings such as tight cracks or fatigue cracks of hairline type are best detected with penetrant test systems and penetrants easily into the narrow openings.

Fluidity: Ability of a liquid to flow is known as fluidity, the penetrant should have the ability to drain away from the component without dragging its original marks that revealed the defects.

Wettability: It is the ability of a penetrant to wet the surface of the material, it is the measure as the area of contact with the surface. The angle of contact for a penetrant should be less than 5 degrees.

Flash Point: Penetrant should have a high flash point as a matter of safety, flashpoint should be above 93.3°C/200°F.

Some other factors to be considered are chemical composition which should not react with the job surface and harm it, drying characteristics and specific gravity, etc. 

The three major types of penetrants are Visible, Fluorescent and Dual (Fluorescent & Visible) type. The most appropriate penetrant is chosen on the basis of defect Sensitivity required, Job Dimensions, Material of the Job and Surface Condition.

Different types of Penetrants and Selection

Colour Contrast/Visible Dye Penetrant: Visible dye penetrant’s indication can be used in daylight or by artificial white light as it does not require a dark room setup. It is mainly used for large test parts which cannot be moved to a dark room setup and need to be tested remotely. Due to the simple application and no specific setup requirement, they are also cost effective as compared to other available penetrants.

Fluorescent Penetrant: These are mainly used for detection of tight/fine cracks which require fluorescent inspection and can be clearly visible under black/fluorescent light. These are mainly used in Aerospace industry for critical parts.

Dual Purpose Penetrant (Fluorescent/Colour Contrast): Dual purpose penetrant produces indications visible under both black light and natural or artificial white light. The larger flaws are visible under both black light and natural white light which provides two different level of sensitivity. The theory is that the visible non-fluorescent dyes are better able to detect large surface cracks while the fluorescent dyes are more useful in connection with the very fine surface cracks.
Developer Selection
The developer must be adsorptive to maximize blotting with fine grain size and particle shape that will disperse and expose the penetrant at a flaw to produce strong and sharply defined indications of the defect. It must be capable of providing a contrast background for indications with a thin and uniform coating over the job surface. Developer must be non-fluorescent if used with fluorescent penetrants and should be easy to remove after inspection. It must not contain ingredients harmful to parts being inspected or to equipment used in the inspection also must not contain ingredients harmful or toxic to the operator. 

According to ASTM 1417, developers are classified into 4 types, which are dry powder, water soluble, water suspendable & non-aqueous developer.

Dry Powder Developer: Dry powder developer is generally considered to be the least sensitive, but it is inexpensive to use and easy to apply. This developer is applied to dry test part surfaces by air suspension, electrostatic spraying, or part immersion. These are mainly used where indications are required to brighter and more distinct over time. Dry powder developer cannot be used with visible systems as they do not form a contrast background

Aqueous (Water Soluble): Aqueous developer contain wetting agents and soluble developer dissolved in water or solvent which dry to leave thin, uniform developer coating. These developers are used where uniform coating of the whole part is required as the coating is translucent and provides poor contrast, they are not recommended for visible systems.

Water Suspendable: Water suspendable developers consist of insoluble developer particles suspended in water. Here, the indications are bright and sharp and it produces white coating of good contrast which can be utilized for visible as well as penetrant systems.

Non Aqueous: Non aqueous developers are said to provide the highest sensitivity and indications show-up at a faster rate as compared to other developers. These developers work well for both visible as well as fluorescent systems
Cleaner Selection
Solvent Cleaners remove excess surface penetrant through direct solvent action. There are two basic types of solvent removers – Halogenated & Non-Halogenated.

Halogenated: It is non-flammable water-soluble compounds containing specially selected surfactant for wetting, penetrating, emulsifying and saponifying various type of soils such as grease and oily films, cutting and machining fluids and unpigmented drawing compounds. Non-flammable cleaners are widely used. However, they do contain halogenated solvents, which may render them unsuitable for some applications.

Non-Halogenated: It is a flammable solvent remover & can be used on a wide range of substrates to remove oils, grease, wax, and sealants; paints other contaminates. Solvent cleaners are not recommended for removal of rust and scale, welding flux and spatter. Flammable cleaners are essentially free of halogens but are potential fire hazards. Non halogenated cleaner is mostly used in the NDT industry.
International Standards and References:
  • ASTME165: Standard Practice for Liquid Penetrant Examination for General industry.
  • ASTM E1417: Standard Practice for Liquid Penetrant Testing
FlawGlo Series of Liquid Penetrant Testing Chemicals
Salient Features:
  • Vivid, high contrast color
  • Low in Sulphur and halogens
  • Good in Wettability, Viscosity & capillarity
  • Superior flaw resolution
  • Water washable and solvent type penetrant
  • Excellent reliability
  • High flash point
  • Compatible with any metals & many synthetic materials.
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